BL12C High-throughput XAFS

2020/3/9 2024/7/25

Techniques

XAFS(X-ray Absorption Fine Structure)

Energy range: 4 – 20 keV (4 – 6 keV with Mirror)
Transmission mode: QXAFS
Fluorescent mode: Lytle detector, 7-elements Silicon Drift Detector (SDD)

Other experimental with monochromatized X-ray

Please contact us before experiment

Light source

PF Bending magnet #12

Ring energy: 2.5 GeV
Max. current: 450 mA (Usually Top-up operation)
Critical energy: 4 keV
Horizontal acceptance: 2 mrad

Beamline optics

Monochromator

Si(111) Water-cooled double crystal
Energy range: 4 – 20 keV
Cam-drive (Kohzu system)

Focusing system

Bent cylinder mirror (Rh coated)
Standard beam size: 0.6H x 0.6V mm

Others

Double flat morror (Ni coated) for higher harmonics reduction

Performance

Focused and Monochromatized mode

Energy range: 4 – 20 keV
Energy resolution: ΔE/E～2×10^-4
Photon flux at sample position: 9×10¹⁰ phs/s (8 keV)

Experimantal station

Experimental hutch

Hatch size: 3.0L x 3.2W x 2.8H m
Door size: 2.4W x 2.4H m

Standard setup

Flat table size: 1500L x 1000W mm
XAFS setup: Ionization chumber, 7-elements SDD, Cryocooler
Automatic sample changer system (Max. 100 samples)

Highlights

Photon Factory Highlights 2018, 1-8, Experimental Evidence of Orbital Ferrimagnetism by X-Ray Magnetic Circular Dichroism, H. Koizumi, S. Sharmin, K. Amemiya, M. S-Sakamaki, J. Inoue and H. Yanagihara
Photon Factory Highlights 2018, 1-16, Nanoscale Ice-Type Structural Fluctuation in Spinel Titanates, S. Torigoe, T. Hattori, K. Kodama, T. Honda, H. Sagayama, K. Ikeda, T. Otomo, H. Nitani, H. Abe, H. Murakawa, H. Sakai and N. Hanasaki
Photon Factory Highlights 2017, 2-7, Origin of the Blue-Green Light Absorption of Ti-Doped AlN Films, S. Imada, N. Tatemizo, Y. Miura, K. Nishio, T. Isshiki1, S. Hirata, F. Sawa, and K. Fukui
Photon Factory Highlights 2017, 2-8, Structural Analysis of Ultra-Small Metal or Alloy Clusters, T. Imaoka, W.-J. Chun and K. Yamamoto
Photon Factory Highlights 2016, 3-3, Charge Compensation Mechanisms of Li1.2-xTi0.4Me0.4O2 (Me = Mn3+ and Fe3+) on Electrochemical Lithium Extraction, N. Yabuuchi
Photon Factory Highlights 2015, 3-1, Structure of the Most Catalytically Active Platinum Cluster (Pt19), T. Imaoka, W.-J. Chun and K. Yamamoto

Beamline manager

城戸大貴 / KIDO Daiki (KEK-PF)
daiki.kido[@]kek.jp